The method does not count beta particles but the number of carbon atoms present in the sample and the proportion of the isotopes. Samples that have been radiocarbon dated since the inception of the method include charcoal, wood, twigs, seeds, bones, shells, leather, peat, lake mud, soil, hair, pottery, pollen, wall paintings, corals, blood residues, fabrics, paper or parchment, resins, and water, among others.
Physical and chemical pretreatments are done on these materials to remove possible contaminants before they are analyzed for their radiocarbon content.
American physical chemist Willard Libby led a team of scientists in the post World War II era to develop a method that measures radiocarbon activity.
He is credited to be the first scientist to suggest that the unstable carbon isotope called radiocarbon or carbon 14 might exist in living matter. Libby and his team of scientists were able to publish a paper summarizing the first detection of radiocarbon in an organic sample. Libby who first measured radiocarbon’s rate of decay and established 5568 years ± 30 years as the half-life. Libby was awarded the Nobel Prize in Chemistry in recognition of his efforts to develop radiocarbon dating.1.
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When the stocks of Oxalic Acid I were almost fully consumed, another standard was made from a crop of 1977 French beet molasses.
The new standard, Oxalic Acid II, was proven to have only a slight difference with Oxalic Acid I in terms of radiocarbon content.
The principal modern standard used by radiocarbon dating labs was the Oxalic Acid I obtained from the National Institute of Standards and Technology in Maryland. Around 95% of the radiocarbon activity of Oxalic Acid I is equal to the measured radiocarbon activity of the absolute radiocarbon standard—a wood in 1890 unaffected by fossil fuel effects.
Accelerator mass spectrometry (AMS) is a modern radiocarbon dating method that is considered to be the more efficient way to measure radiocarbon content of a sample.
In this method, the carbon 14 content is directly measured relative to the carbon 12 and carbon 13 present. Some inorganic matter, like a shell’s aragonite component, can also be dated as long as the mineral’s formation involved assimilation of carbon 14 in equilibrium with the atmosphere.
Background radiocarbon activity is measured, and the values obtained are deducted from the sample’s radiocarbon dating results.
Background samples analyzed are usually geological in origin of infinite age such as coal, lignite, and limestone.